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Sarah explains whats going on and what to do in her article linked below

Role of reactive oxygen species in epilepsy In: NoebelsJLAvoliMRogawskiMAVezzaniADelgado-EscuetaAV, editors

doi: 10.1126/sciadv.abc9955
STG was positive more often in the exposed group than the control group (17.8 vs 10.9%), and the mean value was 38 times higher in the exposed group (1.75 vs 0.046 ng/g creatinine)

Never freeze reconstituted solution as this destroys the peptide structure
