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Mass Spectrometry High-resolution mass spectrometric analyses (UPLC-ESI-TOF MS) were performed on a Waters Synapt G2-S HDMS spectrometer coupled to an Acquity UPLC core system (Waters, Milford, MA, USA) consisting of a binary solvent manager, sample manager and a 2 150 mm, 1.8 m, HSS T3 C18 column (Waters, Manchester, UK)

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They were randomly assigned in the ratio of 1:1:1 to once-weekly subcutaneous CagriSema (n=31), semaglutide (n=31), or cagrilintide (n=30) (all escalated to 24 mg)